Heated Capillary Plate (code: TCP)

Details

Temperature range covers from 20 - ~350C.

  • Holds capillaries up to 2 mm in diameter, working best for 1.5mm and 2.0mm.
  • Best to fill samples >=20mm.
  • We recommend sealing with Devcon 5 Minute or 2 Ton Epoxy. If you have not used these before, you may need some practice to get a feel for the mixing and hardening times.
  • Works for glass/quartz capillaries and kapton capillaries; quartz capillary is preferred because of its high mechanical strength. Commercial Sources: Hampton | Charles Supper

Notes:

  • For solution samples only, not powders; thick powder samples could saturate detector.
  • Solvents with high-Z element (i.e., chloroform) may not work due to high x-ray absorption.

Experiment

  • Beamline staff will unpack your samples the morning of your experiment and stage them inside the station.
  • Remote operation requires additional instructions and orientation.